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The researchers compared the effectiveness and accuracy of their new method against two established methods, Karl Fischer titration and “loss on drying,” which involves putting the sample in a vacuum oven over a period of hours to measure water content. They found that loss on drying took many hours to complete, where their method could analyze samples in a total of 10 minutes, five minutes to heat the samples before analysis and a five-minute chromatographic run time. this linkAt the same time, Karl Fischer titration produced inaccurate results in many of the samples of household solid pharmaceutical drugs tested, which included vitamin C, Excedrine Migraine medicine, and acetaminophen from Target and Walgreens. In addition, using the Armstrong method, only 10 milligrams of sample was needed due to the high sensitivity of the Shimadzu detector, creating an additional advantage for manufacturers. Ten milligrams is roughly equivalent to a light dusting of powder on a finger tip. Frederick MacDonnell, chair of UTA’s Department of Chemistry and Biochemistry, underlined the importance of this new method to improve drug testing methods as the university increases its focus on Health and the Human Condition within the Strategic Plan 2020: Bold Solutions|Global Impact. “This is an example of where basic research on ionic liquids led to a very practical outcome with clear business implications for the pharmaceutical industry,” MacDonnell said. “This may be the first new method that can really take aim at Karl Fischer titration, which has been the mainstay for measuring water content for more than 80 years.” The new paper builds on a initial research published in The Journal of Pharmaceutical and Biomedical Analysis in 2014 that focused on measuring water content in active pharmaceutical ingredients. Armstrong has been a leader in characterizing and synthesizing ionic liquids.
For the original version including any supplementary images or video, visit Cheaper, faster, more accurate method to quantify water in solid pharmaceutical drugs | EurekAlert! Science News
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